Validation of a 1D 1H-NOESY experiment for fingerprinting of grape juices - eBook

Descrizione

Since the first experiments on the detection of nuclear resonance signals, NMR spectroscopy has been successfully used as quantitative technique applied to several kind of matrixes. The recent progress in the development of high sensitive instruments allowed for reduction of the detection limits, thus making the technique appealing also for analysis of molecules in very low concentrations.

Despite the advantages deriving from the use of NMR and despite the plethora of well documented validation processes (e.g., precision, accuracy, linearity, reproducibility, robustness, selectivity, and specificity), very few official NMR based quantification methods are known.

With the aim to encourage the use of quantitative NMR in official methods, Innovative Solutions embarked in the organization of NMR interlaboratory comparisons (NMR-ILCs) according to ISO/IEC 17043:2010 and reference normative therein. NMR-ILCs provide objective standards for individual laboratories, allow them to compare analytical results from different laboratories and represent a way to check the quality and the accuracy of the analytical job.

Results of the NMR-ILCs organized by Innovative Solutions are published in the series “NMR Interlaboratory Comparisons”.

In the present volume, a fingerprinting method for characterization of wine grape juice is considered. The comparison is organized and funded by Innovative Solutions S.r.l. in the framework of the project “Recupero del Germoplasma Viticolo Pugliese” (Re.Ge.Vi.P.), “Progetti Integrati per la Biodiversità” – P.S.R. FEASR 2014-2020, Misura 10.2.1 “Progetti per la conservazione e valorizzazione delle risorse genetiche in agricoltura” – Trascinamento della Mis. 214 Az. 4 sub az. a) del PSR 2007-2013.

Vito Gallo Nicola Intini Piero Mastrorilli Mario Latronico Stefano Todisco Antonino Rizzuti Rosa Ragone Pasquale Scapicchio Paolo Dambruoso Mauro Andrea Cremonini Francesca Benevelli Stefano Ghelli